Korean Journal of Chemical Engineering, Vol.32, No.12, 2512-2518, 2015
Fine control of particle size by seeding and ageing under agitation in the synthesis of analcime zeolite
The size of analcime particles produced through hydrothermal reactions of alkaline synthesis mixtures was finely controlled by seeding and ageing under agitation. Adding acid-treated analcime seeds to the synthesis mixture followed by ageing in an agitated vessel facilitated further nucleation, which resulted in the formation of fine analcime particles with an extremely narrow size distribution. The size of analcime particles could be controlled in the range of 0.5-5.0 μm with a standard deviation of less than 0.1 μm by varying the amount and type of the acid-treated seeds, the ageing time, and the agitation speed.
[References]
Barrer RM, Hydrothermal chemistry of zeolites, Academic Press, London (1982).
Breck DW, Zeolite molecular sieves, John Wiley & Sons, New York (1974).
Szostak R, Molecular sieves: Principles of synthesis and identification, Van Nostrand Reinhold, New York (1989).
Robson H, Ed., Verified syntheses of zeolitic materials, Elsevier, Amsterdam (2001).
Zhdanov SP, Khvoshchev SS, Feoktistova NN, Synthetic zeolites, Gordon and Breach Science Publishers, Amsterdam (1990).
Jihong Y, in Introduction to zeolite science and practice, Cejka J, Bekkum H, Corma A, Schuth F, Eds., Elsevier, Amsterdam (2007).
Park SE, Jiang N, in Zeolites and catalysis, Cejka J, Corma A, Zones S, Eds., WILEY-VCH, Weinheim (2010).
Tosheva L, Valtchev VP, Chem. Mater. , 17 , 2494, 2005
Brar T, France P, Smirniotis PG, Ind. Eng. Chem. Res. , 40 (4), 1133, 2001
Wang C, Li J, Yan J, Sun J, Korean J. Chem. Eng. , 31 (9), 1547, 2014
Ko YS, Ahn WS, Korean J. Chem. Eng. , 25 (6), 1546, 2008
Sharma P, Rajaram P, Tomar R, J. Colloid Interface Sci. , 325 (2), 547, 2008
Di Renzo F, Catal. Today , 41 (1-3), 37, 1998
Wiersema GS, Thompson RW, J. Mater. Chem. , 6 , 1693, 1996
Cundy CS, Cox PA, Microporous Mesoporous Mater. , 82 , 1, 2005
Subotic B, Bronic J, in Handbook of zeolite science and technology, Auerbach SM, Carrado KA, Dutta PK, Eds., Marcel Dekker, New York (2003).
Lee CH, Park SW, Kim SS, Korean J. Chem. Eng. , 31 (2), 179, 2014
Kaeding WW, J. Catal. , 95 , 512, 1985
Lee KY, Chae HJ, Jeong SY, Seo G, Appl. Catal. A: Gen. , 369 (1-2), 60, 2009
Thompson RW, in Molecular sieves: Synthesis, Karge HG, Weitkamp J, Eds., Springer, New York (1998).
Majano G, Darwiche A, Mintova S, Valtchev V, Ind. Eng. Chem. Res. , 48 (15), 7084, 2009
Ren N, Yang ZJ, Lv XC, Shi J, Zhang YH, Tang Y, Microporous Mesoporous Mater. , 131 , 103, 2010
Park SH, Chung CB, Seo G, Microporous Mesoporous Mater. , 155 , 201, 2012
Treacy MMJ, Higgins JB, Collection of simulated XRD powder patterns for zeolites, Elsevier, New York (2007).
Pan Y, Ju M, Yao J, Zhang L, Xu N, Chem. Commun. , 46 , 7233, 2009
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