Korean Journal of Chemical Engineering, Vol.37, No.6, 1097-1106, 2020
A facile method to synthesize magnetic nanoparticles chelated with Copper(II) for selective adsorption of bovine hemoglobin
A novel and uncomplicated synthesis method of Cu2+-chelating with carboxyl groups that directly-modified NiFe2O4 magnetic microspheres (NiFe2O4-PAA-Cu2+) was fabricated for selective enrichment and separation of bovine hemoglobin (BHb). First, a carboxyl group directly-modified on NiFe2O4 magnetic microspheres was gained through a facile one-pot solvothermal method. Second, Cu2+ from CuSO4 was brought into use to react with carboxyl groups under mechanical stirring at room temperature. The resulting magnetic microspheres were characterized by distinct instruments that included transmission electron microscopy (TEM), Brunauer-Emmett-Teller (BET), Fourier transform infrared spectroscopy (FT-IR), X-ray photoelectron spectroscopy (XPS), vibrating sample magnetometer (VSM) and scanning electron microscope (SEM) to examine the size, morphology, composition and magnetization characterization. The results indicated that the NiFe2O4-PAA-Cu2+ microspheres exhibited good saturation magnetization(36.686 emu g?1), which can facilitate magnetic separation under the help of an outside magnetic field. Also, good dispersion and high adsorption ability to BHb (783.53mg g?1) can be applied to selective enrichment for bovine hemoglobin and used for selective sorption of BHb protein in bovine blood samples.
[References]
Zhai QZ, Zhang XX, Asian J. Chem. , 20 , 5060, 2008
Wang BH, Shao Q, New J. Chem. , 41 , 5651, 2017
Graves DJ, Trends Biotechnol. , 17 , 127, 1999
Wang YQ, Zhang HM, Int. J. Biol. Macromol. , 41 , 243, 2007
Liu YJ, Wang YZ, Anal. Chim. Acta , 936 , 168, 2016
Li DY, Wang YZ, J. Mater. Chem. B , 2 , 5659, 2014
Tetala KKR, Skrzypek K, Levisson M, Stamatialis DF, Sep. Purif. Technol. , 115 , 20, 2013
Wang JD, Tan SY, Talanta , 190 , 210, 2018
Din C, Ma XD, J. Chromatogr. A , 1424 , 18, 2015
Liu BS, Yang XN, Luminescence , 29 , 211, 2014
Guo ZY, Zhang Y, ACS Appl. Mater. Interfaces , 8 , 29734, 2016
Wuenschell GE, Naranjo E, Arnold FH, Bioprocess Eng. , 5 , 199, 1990
Zhang Y, Xing LG, ACS Appl. Mater. Interfaces , 7 , 5116, 2015
Zhai Q, Zhang X, Asian J. Chem. , 20 , 5060, 2008
Mu PQ, Feng DR, J. Biochem. , 150 , 491, 2011
Wang JJ, Zhang R, Talanta , 176 , 308, 2018
Du KF, Liu XH, ACS Sustainable Chem. Eng. , 6 , 11578, 2018
Kip C, Tosunb RB, Talanta , 200 , 100, 2019
Guo ZY, Zhang Y, ACS Appl. Mater. Interfaces , 8 , 29734, 2016
Zhang Y, Xing LG, ACS Appl. Mater. Interfaces , 7 , 5116, 2015
Guo TY, Xia YQ, Biomaterials , 25 , 5905, 2004
Jia XP, Xu ML, Analyst , 138 , 651, 2013
Kan XW, Zhao Q, Shao DL, Geng Z, Wang ZL, Zhu JJ, J. Phys. Chem. B , 114 (11), 3999, 2010
Yang XD, Zhang M, Zheng J, Li WZ, Gan WJ, Xu JL, Hayat T, Alharbi NS, Yang F, Appl. Surf. Sci. , 439 , 128, 2018
Zhang M, He XW, Nanotechnology , 22 , 065705, 2011
Zhang M, He XW, J. Mater. Chem. , 20 , 10696, 2010
Zhang H, Wang WW, New J. Chem. , 42 , 3990, 2018
Zheng JN, Lin Z, J. Mater. Chem. B. , 2 , 6207, 2014
Zhang YW, Zhang M, J. Alloy. Compd. , 695 , 3256, 2017
Zheng JN, Lin Z, J. Mater. Chem. B. , 3 , 2185, 2015
Gomez B, Rubio S, Anal. Chem. , 81 , 9012, 2009
Deng H, Li X, Peng Q, Angew. Chem. , 117 , 2842, 2005
Deng YH, Deng CH, Qi DW, Liu C, Liu J, Zhang XM, Zhao DY, Adv. Mater. , 21 (13), 1377, 2009
Niasari MS, Davar F, Polyhedron , 28 , 1455, 2009
Hu YZ, Zhao CF, Yin L, Wen T, Yang Y, Ai YJ, Wang XK, Chem. Eng. J. , 349 , 347, 2018
Mirahmadi-Zare SZ, Allafchian A, Protein Expression and Purification, 121, 52 (2016).
Li JH, Chen MJ, Colloids Surf. B: Biointerfaces , 146 , 468, 2016
Wan W, Liang QL, Analyst , 141 , 4568, 2016
Lu AH, Salabas EL, Angew. Chem.-Int. Edit. , 46 , 1222, 2007
Faraji M, Yamini Y, Chem. Soc. , 7 , 1, 2010
Salimi K, Usta DD, RSC Adv. , 7 , 8718, 2017
Zhao M, Deng CH, Chem. Commun. , 50 , 6228, 2014
Yao X, Ma XD, RSC Adv. , 7 , 29330, 2017
Zhang M, Wang YT, Zhang YW, Ding L, Zheng J, Xu JL, Appl. Surf. Sci. , 375 , 154, 2016
Block H, Maertens B, Methods Enzymol. , 463 , 440, 2009
Maensiri S, Masingboon C, Scripta Mater. , 56 , 797, 2007
Sivakumar P, Ramesh R, Mater. Res. Bullet. , 46 , 2204, 2011
Cheng YL, Zhao Y, Zhang YF, Cao XQ, J. Colloid Interface Sci. , 344 (2), 321, 2010
Kurtana U, Gungunes H, Ceram. Int. , 42 , 7987, 2016
Yue Q, Li JL, Luo W, Zhang Y, Elzatahry AA, Wang XQ, Wang C, Li W, Cheng XW, Alghamdi A, Abdullah AM, Deng YH, Zhao DY, J. Am. Chem. Soc. , 137 (41), 13282, 2015
Rouquerol F, Rouquerol J, Adsorption by powders and porous solids: principles, methodology and applications, 2nd Ed., Elsevier, Amsterdam, 11 (2014).
Zhang Y, Guo ZY, Carbon , 122 , 194, 2017
Satyanarayana L, Reddy KM, Manorama SV, Mater. Chem. Phys. , 82 (1), 21, 2003
Liu J, Bin YZ, J. Phys. Chem. C , 116 , 134, 2012
Jian GQ, Liu YX, Nanoscale , 4 , 6336, 2012
Gao RX, Cui XH, Talanta , 150 , 46, 2016
Liu YJ, Wang YZ, Anal. Chim. Acta , 936 , 168, 2016
Zhang M, Cheng D, Asian J. , 5 , 1332, 2010
Gao RX, Mu XR, J. Mater. Chem. B. , 2 , 1733, 2014
Wang JD, Guan HY, ACS Biomater. Sci. Eng. , 5 , 2740, 2019
Altıntas EB, Turkmen D, Colloids Surf. B: Biointerfaces , 85 , 235, 2011
Zhang Y, Xing LG, ACS Appl. Mater. Interfaces , 7 , 5116, 2015
Shi L, Tang YH, J. Sep. Sci. , 39 , 2876, 2016
이전 논문 다음 논문
Result Search