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Received July 8, 2018
Accepted December 18, 2018
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Synthesis and performance evaluation of zeolitic imidazolate framework-8 membranes deposited onto alumina hollow fiber for desalination
Nizar Mu’ammar Mahpoz
Norfazliana Abdullah
Mohamad Zahir Mohd Pauzi
Mukhlis A. Rahman1†
Khairul Hamimah Abas2
Azian Abd Aziz3
Mohd Hafiz Dzarfan Othman
Juhana Jaafar
Ahmad Fauzi Ismail
Universiti Teknologi Malaysia, Advanced Membrane Technology Research Centre (AMTEC), 81310 Skudai, Johor, Malaysia 1Advanced Membrane Technology Research Centre (AMTEC), Universiti Teknologi Malaysia 81310 Skudai, Johor, Malaysia 2Department of Control & Instrumentation Engineering, Faculty of Electrical Engineering, Universiti Teknologi Malaysia, 81310 Skudai, Johor, Malaysia 3Language Academy, Universiti Teknologi Malaysia, 81310 Skudai, Johor, Malaysia
Korean Journal of Chemical Engineering, March 2019, 36(3), 439-449(11), 10.1007/s11814-018-0214-6
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Abstract
This work describes the development of zeolitic imidazolate framework-8 (ZIF-8) membranes on modified alumina hollow fiber for desalination by forward osmosis. Effects of different seeds (ZnO, NiO and PDA) and sodium formate on in-situ deposition of ZIF-8 were studied in relation to the membrane…s morphology and performance. XRD result shows that ZIF-8 was successfully synthesized in the presence of sodium formate. FESEM images showed PDA modified support was unsuccessful in producing well defined and dense ZIF-8 membrane layer even after another ZIF-8 re-deposition due to its minimal amount. The NiO modified support was also found unsuccessful, as ZIF-8 crystals were formed in clusters. On the contrary, dense ZIF-8 membrane was successfully prepared on ZnO modified support with SF-1 synthesis solution producing bigger ZIF-8 crystal and thinner ZIF-8 membrane than as of SF-2. Water flux performance in forward osmosis showed that NiO/ZIF-8, PDA/ZIF-8 and PDA/ZIF-8 (re-deposition) membranes gave negative water fluxes of -50 kg/m2ㆍh, -5.2 kg/m2ㆍh and -1.7 kg/m2ㆍh with reverse solutes of 42.66 mol/m2ㆍh, 27.42mol/m2ㆍh and 3.22 mol/m2ㆍh, respectively, indicating the solute from draw solution diffused into the feed solution. However, ZIF-8 membrane prepared using SF with molar ratio of 1, on the ZnO modified support had a water flux of 13.3 kg/m2ㆍh, reverse solute of 0.95 kg/m2ㆍh and salt rejection of 52.1%. When the SF ratio was increased to 2, the ZIF-8 membranes showed a water flux of 12.5 kg/m2ㆍh, reverse solute of 1.64 kg/m2ㆍh and salt rejection of 54.9%. The moderate salt rejection could be associated with defects in the ZIF-8 membranes due to poor grain boundaries.
Keywords
References
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Mcguire CV, Forgan RS, Chem. Commun., 51, 5199 (2014)
Cravillon J, Nayuk R, Springer S, Feldhoff A, Huber K, Wiebcke M, Chem. Mater., 23, 2130 (2011)
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Gupta KM, Zhang K, Jiang JW, Langmuir, 31(48), 13230 (2015)
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Fairen-Jimenez D, Moggach SA, Wharmby MT, Wright PA, Parsons S, Duren T, J. Am. Chem. Soc., 133(23), 8900 (2011)
