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Received April 22, 2016
Accepted August 2, 2016
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Immobilization of the Thenoyltrifluoroacetone on Sodium Dodecyl Sulfate Modified Magnetite Nanoparticles for Magnetic Solid Phase Extraction of Pb (II) from Water Samples
Young Researchers and Elite Club, Ahvaz Branch, Islamic Azad University, Ahvaz, Iran 1Department of Chemistry, Faculty of Basic Sciences, Islamic Azad University, Qaemshahr Branch, Qaemshahr, Iran 2Department of Applied Chemistry, Faculty of Pharmaceutical Chemistry, Pharmaceutical Sciences Branch, Islamic Azad University, Tehran, Iran
Korean Chemical Engineering Research, October 2016, 54(5), 636-647(12), 10.9713/kcer.2016.54.5.636 Epub 6 October 2016
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Abstract
Magnetite nanoparticles (Fe3O4 NPs) were synthesized by co-precipitating method under optimized condition. The Fe3O4 NPs coated with sodium dodecyl sulfate-thenoyltrifluoroacetone (Fe3O4 NPs-SDS-TTFA) were then exerted as the magnetic solid phase extraction (MSPE) adsorbent for the extraction process prior to introducing to a flame atomic adsorption spectrometry (FAAS). The synthesized Fe3O4 NPs-SDS-TTFA were applied for the extraction of Pb(II) ions from different water samples. The characterization studies of nanoparticles were performed via scanning electron microscopy-energy dispersive micro-analysis (SEM-EDAX), X-ray diffraction (XRD) and vibrating sample magnetometer (VSM) techniques. The substantial parameters affecting the extraction efficiency were surveyed and optimized. A dynamic linear range (DLR) of 10.400 μg L-1 was obtained and the limit of detection (LOD, n=7) and relative standard deviation (RSD%, n= 6, C=20 μg L-1) were found to be 2.3 μg L-1 and 1.9%, respectively. According to the results, the proposed method successfully applied for the extraction of Pb(II) ions from different environmental water samples and satisfactory results achieved.
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References
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Baytak S, Turker AR, J. Hazard. Mater., 129(1-3), 130 (2006)
Wang ZY, Su YD, Li S, Spectrosc. Spect. Anal., 28(11), 2695 (2008)
Tavallali H, Asrari E, Attaran A, Tabandeh M, Int. J. Chem. Tech. Res., 2(3), 1731 (2010)
Panda L, Das B, Rao DS, Korean J. Chem. Eng., 28(10), 2024 (2011)
Mahmoud ME, Yakout AAA, Abdel H, Osman MM, Bioresour. Technol., 106(1), 125 (2012)
Bouranene S, Fievet P, Szymczyk A, Samar MEH, Vidonne A, J. Membr. Sci., 325(1), 150 (2008)
Ghaedi M, Shokrollahi A, Niknam K, Niknam E, Najibi A, Soylak M, J. Hazard. Mater., 168(2-3), 1022 (2009)
Citak D, Tuzen M, Food. Chem. Toxicol., 48(5), 1399 (2010)
Comitre ALD, Reis BF, Talanta, 65(4), 846 (2005)
Liang P, Sang H, Anal. Biochem., 380(1), 21 (2008)
Rivas RE, Lopez GI, Hernandez CM, Microchim. Acata., 166(3), 355 (2009)
Zhang L, Chang X, Li Z, He Q, J. Mol. Struct., 964(1-3), 58 (2010)
Bai H, Zhou Q, Xie G, Xiao J, Talanta, 80(5), 1638 (2010)
Baysal A, Kahraman M, Akman S, Curr. Anal. Chem., 5(4), 352 (2009)
Parham H, Pourreza N, Rahbar N, J. Hazard. Mater., 163(2-3), 588 (2009)
Qiu G, Wang Q, Wang C, Lau W, Guo Y, Ultrason. Sonochem., 14(1), 55 (2007)
Bhaumik M, Maity A, Srinivasu VV, Onyango MS, J. Hazard. Mater., 190(1-3), 381 (2011)
Tataru G, Popa M, Desbrieres J, Int. J. Pharm., 404(1-2), 83 (2011)
Kalfa OM, Yalcinkaya O, Turker AR, J. Hazard. Mater., 166(1), 455 (2009)
Singh S, Barick KC, Bahadur D, J. Hazard. Mater., 192(3), 1539 (2011)
Izatt RM, Bradshaw JS, Bruening RL, Pure. Appl. Chem., 68(1), 1237 (1996)
Suh YJ, Do TM, Kil DS, Jang HD, Cho K, Korean Chem. Eng. Res., 53(1), 39 (2015)
Akama Y, Ito M, Tanaka S, Talanta, 53(3), 645 (2000)
Khajeh M, Laurent S, Dastafkan K, Chem. Rev., 113(10), 7728 (2013)
Acar HYC, Garaas RS, Syud F, Bonitatebus P, Kulkarni AM, J. Magn. Magn. Mater., 293(1), 1 (2005)
Jeng HT, Guo GY, Phys. Rev. B, 65(9), 094429 (2002)
Tartaj P, del Puerto MM, Veintemillas-Verdaguer S, Gonzalez-Carreno T, Serna C, J. Phys. D-Appl. Phys., 36(13), 182 (2003)
Cornell RM, Schwertmann U, Iron oxides: Structure, Properties, Reactions, Occurrence, and Uses, 2nd ed.,Wiley-VCH, Weinheim(2003).
Muller R, Dutz S, Habisreuther T, Zeisberger M, J. Magn. Magn. Mater., 323(10), 1223 (2011)
Kassaee MZ, Motamedi E, Majdi M, Chem. Eng. J., 172(1), 540 (2011)
Zhang J, Zhai S, Li S, Xiao Z, Song Y, Qingda A, Tian G, Chem. Eng. J., 215-216(1), 461 (2013)
Sun ZX, Su FW, Forsling W, Samskog PO, J. Colloid Interface Sci., 197(1), 151 (1998)
Tan Y, Chen M, Hao Y, Chem. Eng. J., 191(1), 104 (2012)
Karimi MA, Hatefi-Mehrjardi A, Mohammadi SZ, Mohadesi A, Mazloum-Ardakani M, Hormozi Nezhad MR, Askarpour Kabir A, J. Iran. Chem. Soc., 9(2), 171 (2012)
Mashhadizadeh MH, Amoli-Diva M, Shapouri MR, Afruzi H, Food Chem., 151(1), 300 (2014)
Buendia S, Cabanas G, Alvarez-Lucio G, Montiel-Sanchez H, Navarro-Clemente ME, Corea M, J. Colloid Interface Sci., 354(1), 139 (2011)
Tarley CRT, Ferreira SLC, Arruda MAZ, Microchem J., 77(2), 163 (2004)
Patterson A, Phys. Rev., 56(10), 978 (1939)
Ngomsik AF, Bee A, Siaugue JM, Talbot D, Cabuil V, Cote G, J. Hazard. Mater., 166(2-3), 1043 (2009)
Saracoglu S, Elci L, Anal. Chim. Acta., 452(1), 77 (2002)
Ferreira SLC, lemos VA, Santelli RE, Ganzarolli E, Curtius AJ, Microchem J., 68(1), 41 (2001)
Costa ACS, Lopesa L, Korn MGA, Portela JG, J. Braz. Chem. Soc., 13(5), 674 (2002)
Ozmen M, Can K, Arslan G, Tor A, Cengeloglu Y, Ersoz M, Desalination, 254(1-3), 162 (2010)
Zhu X, Chang X, Cui Y, Zou X, Yang D, Hu Z, Microchem J., 86(2), 189 (2007)
Candir S, Narin I, Soylak M, Talanta, 77(1), 289 (2008)
Singh BK, Kumar DN, Garg BS, Indian J. Chem. Technol., 12(4), 413 (2005)
Sacmaci S, Kartal S, Sacmaci M, Fresen. Environ. Bull., 21(6a)
Moghimi A, Hashemi-Moghaddam H, J. Chem. Health Risks., 5(2), 105 (2015)
Rahnama R, Ghadiri R, J. Braz. Chem., 26(8), 1642 (2015)
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Divrikli U, Kartal AA, Soylak M, Elci L, J. Hazard. Mater., 145(3), 459 (2007)
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Venkatesh G, Singh AK, Venkataramani B, Microchim. Aata., 144(4), 233 (2004)
Mansour SF, J. Magn. Magn. Mater., 323(13), 1735 (2011)
