Korean Journal of Chemical Engineering, Vol.22, No.3, 399-405, 2005
Extraction of Lipids and Cholesterol from Squid Oil with Supercritical Carbon Dioxide
The oil obtained from waste squid viscera consists of multi-compounds such as EPA, DHA and other valuable polyunsaturated fatty acids. The refining of this squid oil, using supercritical carbon dioxide plus ethanol, was performed in a semi-continuous flow extractor at 8 to 17 MPa and 25 to 50 ℃. When 1.5% w/w ethanol was added to the solvent, the solubility of lipids was increased by up to 50% over the neat CO2 value. The extraction curves indicated mass transfer to be solubility limited. Cholesterol was co-extracted with the lipids but, with its lower solubility, less than 54% appeared in the refined oil. The results of the carbon dioxide/multi-compound squid oil system at applied to the extraction conditions were correlated with the mole fraction of the cholesterol and the density of the pure solvent.
[References]
Ackman RG, "The Year of Fish Oils", Chem. and Ind., Mar, 139, 1988
Ackman RG, "Problems in Fish Oils and Concentrates, in Fats for the Future", R. C. Cambie(Ed.), Ch.,, 13 , 189, 1989
Ackman RG, Ratnayake WMN, Macpherson EJ, J. Am. Oil Chem. Soc. , 66 , 1162, 1989
Baek JK, Kim S, Lee GS, Shim JJ, Korean J. Chem. Eng. , 21 (1), 230, 2004
Bandarra MM, Nunes ML, Campos RM, Batista I, Variacao Sazonal dos Lipidos de Sardinha sardinapilchardus. Relatorio Tecnico e Cientifico, 1992
Bulley NR, Labay L, Amtfield SD, J. Supercrit. Fluids , 5 , 13, 1992
Chrastil J, J. Phys. Chem. , 86 , 3016, 1982
Chun BS, Wilkinson GT, J. Chem. Eng. , 16 , 187, 1999
Coenen H, Kriegel E, Ger. Chem. Eng. , 7 , 335, 1984
Dziezak JD, Food Technol. , 40 , 66, 1986
Eisenbach W, Gottsch PJ, Niemann K, Zosel K, Fluid Phase Equilib. , 10 , 315, 1983
Foster, Singh NR, Jimmy H, Yun SL, Tomasko DL, Macnaughton SJM, Ind. Eng. Chem. Res. , 32 , 2849, 1993
Grimmett C, Chem. Ind. , 15 , 359, 1982
Hardardottir I, Kinsella JE, J. Food Sci. , 53 , 1656, 1988
Hartono R, Mansoori GA, Suwono A, Chem. Eng. Sci. , 56 (24), 6949, 2001
Hong IK, RHO SW, LEE KS, LEE WH, YOO KP, Korean J. Chem. Eng. , 7 (1), 40, 1990
Iwai Y, Koga Y, Maruyama H, Arai Y, J. Chem. Eng. Data , 38 , 506, 1993
Karmali RA, Marsh J, Fuchs C, J. Nat. Cancer Inst. , 75 , 457, 1984
Kim EM, Jo JH, Oh SW, Kim YM, J. Korea Fish. Soc. , 30 , 595, 1997
Kosal E, Lee CH, Holder GD, J. Supercrit. Fluids , 5 , 169, 1992
Lands WEM, Fish and Human Health, Academic Press, Inc. Orlando, 1986
Mansoori GA, Schultz K, Martinelli EE, Biomed. Tech. , 6 , 393, 1988
McHugh MA, Krukonis VJ, V. J., Supercritical Fluid Extraction Principles and Practice, Butterworth-Heinemann, 1986
Mohamed RS, Neves GM, Kieckbusch TG, Int. J. Food Sci. Technol. , 33 , 245, 1998
Nilsson WB, Gauglitz EJ, Hudson JK, Stout VF, J. Am. Oil Chem. Soc. , 65 , 109, 1988
Noh MJ, Kim TG, Hong IK, Yoo KP, Korean J. Chem. Eng. , 12 (1), 48, 1995
Rambjor GS, Walen AI, Windsor SL, Harris WS, Lipids , 31 , 45, 1996
Stahl E, Quirin KW, Gerard D, Dense Gases for Extraction and Refining, Chap. IV. Springer-Verlag, New York, 1988
Valderrama JO, Silva A, Korean J. Chem. Eng. , 20 (4), 709, 2003
[Cited By]
Kang DH, Jeh EJ, Seo JW, Chun BH, Hur BK, Korean Journal of Chemical Engineering , 24 (4), 651, 2007
Akman U, Okay N, Oner Hortacsu O, Korean Journal of Chemical Engineering , 25 (2), 329, 2008
Jeh EJ, Kumaran RS, Hur BK, Korean Journal of Chemical Engineering , 25 (5), 1103, 2008
Charoenchaitrakool M, Trisilanun W, Srinopakhun P, Korean Journal of Chemical Engineering , 27 (3), 950, 2010
Kwon KT, Uddin MS, Jung GW, Sim JE, Lee SM, Woo HC, Chun BS, Korean Journal of Chemical Engineering , 28 (6), 1433, 2011
Lee SM, Yun JH, Chun BS, Clean Technology , 17 (3), 266, 2011
Jung GW, Kang HM, Chun BS, Journal of Industrial and Engineering Chemistry , 18 (1), 360, 2012
Davoodi P, Ghoreishi SM, Hedayati A, Korean Journal of Chemical Engineering , 34 (3), 854, 2017
Park JS, Cho YJ, Jeong YR, Chun BS, Clean Technology , 25 (4), 275, 2019
이전 논문 다음 논문
Result Search