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Issue
Korean Journal of Chemical Engineering,
Vol.37, No.12, 2216-2224, 2020
Simultaneous biosynthesis of reduced graphene oxide-Ag-Cu2O nanostructures by lichen extract for catalytic reduction of textile dyes
Ciplak Z, Getiren B, Gokalp C, Dincer CA, Yildiz A, Yildiz N
Metal/metal oxide nanostructures based reduced graphene oxide (LrGO-Ag, LrGO-Cu2O, LrGO-Ag-Cu2O) nanocomposites were obtained via green method using Cetraria islandica (L.) Ach. lichen extract. Fourier transform infrared (FTIR) spectroscopy, transmission electron microscopy (TEM), scanning electron microscope energy-dispersive X-ray spectroscopy (SEM-EDX), ultraviolet-visible (UV-Vis) spectroscopy, X-ray diffraction (XRD) and X-ray photoelectron spectroscopy (XPS) were performed to analyze the prepared nanostructures. The results indicated that thenanocomposites were synthesized effectively and Ag-Cu2O nanoparticles with the mean diameter of 27nm were well dispersed on the LrGO. The conversion of methylene blue (MB) to Leuco Methylene Blue (LMB) and 4-Nitrophenol (4- NP) to 4-Aminophenol (4-AP) was performed by biosynthesized catalysts in the presence of NaBH4. The reaction rate of LrGO-Ag-Cu2O nanocomposite during 4-NP and MB reduction was found as 0.0026 s-1 and 0.0497 s-1, respectively. The LrGO-Ag-Cu2O nanocomposite showed superior catalytic performance for the reduction of both textile dyes.
Keywords: Metal/Metal Oxide Nanostructures; Reduced Graphene Oxide (rGO); Cetraria islandica (L.) Ach. Extract; Green Synthesis; Catalytic Reduction
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