About The Journal
  Aims and Scope
  Editorial Board
  Submit a Manuscript 
  Subscription Information
  Guidelines for Publication
  Ethics
Articles & Issues
  Search
  Issue
  Online First
  KJChE on
For Authors
  Instructions to Authors
  Ethical Responsibilities of
  Authors in KJChE
  Ethics in Publishing
  Peer Review Process
  Author's Checklist
  Copyright Transfer Form
Contact us
 
 
 
Issue
Korean Journal of Chemical Engineering,
Vol.36, No.11, 1869-1881, 2019
Rapid synthesis of phytogenic silver nanoparticles using Clerodendrum splendens: its antibacterial and antioxidant activities
Jayakumar A, Vedhaiyan RK
Silver nanoparticles (AgNPs) were rapidly green synthesized using Clerodendrum splendens (C. splendens) leaf extract with an environment-friendly approach. The stability, morphology and grain size of the AgNPs were determined using Zeta potential analysis, Transmission electron microscopy (TEM) and X-ray diffraction spectra (XRD). The phytochemicals present in the C. splendens, which are responsible for the bioreduction of silver ions (Ag+ ions) and stabilization of AgNPs, were investigated using Fourier transform infrared spectroscopy (FTIR). The vital compositions in the AgNPs solution were analyzed by energy dispersive X-ray spectroscope (EDS). Using X-ray photoelectron spectroscope (XPS) measurement, the effect of C. splendens extract on the formation of AgNPs was investigated. The surface area of the AgNP was evaluated by using multiple point Brunauer-Emmett-Teller (BET) method. Results indicated that a low concentration of leaf extract is enough to enhance the rate of formation of AgNPs. C. splendens instantaneously reduced Ag+ to AgNPs to reach 98% yield within 15 min. The fabricated AgNPs are in the size range of ~46 nm, well crystallized with face-centered cubic (fcc) symmetry. The AgNPs revealed a significant antimicrobial activity against airborne pathogens such as Pseudomonas aeruginosa (P. aeruginosa) and Bacillus subtilis (B. subtilis).
Keywords: Silver Nanoparticles; Clerodendrum splendens; Leaf Extract; Antibacterial; Antioxidant
[References]
  1. Sahoo SK, Misra R, Parveen S, In Nanomedicine in Cancer, 73 (2017).
  2. Shiju NR, Guliants VV, Appl. Catal. A: Gen., 356(1), 1, 2009
  3. Ju-Nam Y, Lead JR, Sci. Total Environ., 400, 396, 2008
  4. Zhang XF, Liu ZG, Shen W, Gurunathan S, Int. J. Mol. Sci., 17, 1534, 2016
  5. Duan H, Wang D, Li Y, Chem. Soc. Rev., 44, 5778, 2015
  6. Prabhu S, Poulose EK, Int. Nano Lett., 2, 32, 2012
  7. Shrestha R, Joshi DR, Gopali J, Piya S, Nepal J. Sci. Technol., 10, 189, 2009
  8. Chahardoli A, Karimi N, Fattahi A, Adv. Powder Technol., 29(1), 202, 2018
  9. Balamurugan M, Saravanan S, J. Inst. Eng. India Ser. A, 98, 461, 2017
  10. Kumar M, Sinha MP, Not. Sci. Biol., 9, 443, 2017
  11. Elumalai D, Hemavathi M, Deepaa CV, Kaleena PK, Parasite Epidemiol. Control, 2, 15, 2017
  12. Asha S, Thirunavukkarasu P, Rajeshkumar S, Int. J. Pharmaceut. Res., 9, 32, 2017
  13. Das K, Tiwari RKS, Shrivastava DK, J. Med. Plants Res., 4, 104, 2010
  14. Ingole SN, Biodiversitas, 12, 146, 2011
  15. Jai RK, Adv. Bio. Res., 1, 84, 2010
  16. Shehata AH, Yousif MF, Soliman GA, Egypt J. Biomed. Sci., 7, 145, 2001
  17. Mshana NR, Abbiw DK, Addae-Mensah I, Adjanohoun E, et al., Organization of African Unity/Scientific, Technical & Research Commision, Accra. (2000).
  18. Burkill HM, The useful plants of west tropical Africa Royal Botanic Gardens. Kew, UK, 130 (1985).
  19. Gbedema SY, Emelia K, Francis A, Kofi A, Eric W, Pharmacognosy Res., 2, 63, 2010
  20. Ahmed S, Swami L, Ikram S, J. Radiat. Res. Appl. Sci., 9, 1, 2016
  21. Brand-Williams W, Cuvelier ME, LWT-Food Sci. Technol., 28, 25, 1995
  22. Kumar T, Jain V, Scientifica, 2015, 1, 2015
  23. Jeyaraj M, Rajesh M, Arun R, Mubarak Ali D, Sathishkumar G, Sivanandhan G, Dev GK, Manickavasagam M, Colloids Surf. B: Biointerfaces, 102, 708, 2013
  24. Noginov M, Zhu G, Bahoura M, Adegoke J, Small C, Ritzo BA, Drachev VP, Shalaev VM, Appl. Phys. B-Lasers Opt., 86, 455, 2007
  25. Clark J, Gunawardena G, The Beer-Lambert Law, Chemistry Libretexts (2016).
  26. Clark J, Absorption spectra- The Beer-Lambert Law, Chemguide (2016).
  27. Ronson K, Nano Composix, 1, 1, 2012
  28. Elbeshehy EK, Elazzazy AM, Aggelis G, Front. Microbiol., 6, 453, 2015
  29. Becue A, Cantu AA, Fingermark detection using nanoparticles, 307 (2012).
  30. Balaji DS, Basavaraja S, Deshpande R, Mahesh DB, Prabhakar BK, Venkataraman A, Colloids Surf. B: Biointerfaces, 68, 88, 2009
  31. Sorokulova IB, Pinchuk IV, Denayrolles M, Osipova IG, Huang JM, Cutting SM, Urdaci MC, Digest. Dis. Sci., 53, 954, 2008
  32. Ogorek R, Lejman A, Pusz W, Milhch A, Miodynska P, Mikol. Pol., 19, 80, 2012
  33. Shareef JU, Rani MN, Anand S, Rangappa D, Mater. Today: Proc., 4, 11923, 2017
  34. Vahabi K, Mansoori GA, Karimi S, Insciences J., 1, 65, 2011
  35. Hashemi S, Givianrad MH, Moradi AM, Larijani K, Indian J. Geo-Mar. Sci., 44, 1415, 2015
  36. Coppen JJ, Eucalyptus: the genus Eucalyptus (2002).
  37. Johnson I, Prabu HJ, Int. Nano Lett., 5, 43, 2015
  38. Agasti N, Am. J. Nanomater., 2, 4, 2014
  39. Cullity BD, Elements of X-ray diffraction (1978).
  40. Fayaz AM, Balaji K, Girilal M, Yadav R, Kalaichelvan PT, Venketesan R, Nanomedicine: NBM, 6, 103, 2010
  41. Michael D, How to Read IR Spectrums, Sciencing (2017).
  42. Kora AJ, Sashidhar RB, Carbohydr. Polym., 82, 670, 2010
  43. Kaviya S, Santhanalakshmi J, Mater. Lett., 67, 64, 2012
  44. Schulz H, Vib. Spectrosc., 43, 13, 2007
  45. Huang J, Li Q, Sun D, Lu Y, Yang X, Wang H, Wang Y, Shao W, He N, Hong J, Nanotechnology, 18, 105104, 2007
  46. Bakhshi H, Yeganeh H, Mehdipour S, Shokrgozar A, Yari A, Saeedi N, Mater. Sci. Eng. C-Biomimetic Supramol. Syst., 33, 153, 2013
  47. Sukirtha R, Priyanka KM, Antony JJ, Kamalakkannan S, Thangam R, Gunasekaran P, Krishnan M, Achiraman S, Process Biochem., 47(2), 273, 2012
  48. Li S, Shen Y, Xie A, Yu X, Qiu L, Green Chem., 9, 852, 2007
  49. Zhang L, Wu Z, Chen L, Zhang L, Li X, Xu H, Wang H, Zhu G, Solid State Sci., 52, 42, 2016
  50. Prasad JS, Dhand V, Himabindu V, Anjaneyulu Y, Int. J. Energy Environ., 1, 607, 2010
  51. Shrivastava S, Bera T, Roy A, Ramachandrarao P, Dash D, Nanotechnology, 18, 225103, 2007
  52. Yen HJ, Hsu SH, Small, 5, 1553, 2009
  53. Dakal TC, Kumar A, Majumdar RS, Front. Microbiol., 7, 1831, 2016
  54. Wang L, Hu C, Int. J. Nanomedicine, 12, 1227, 2017
  55. Fenglin H, Fitoterapia, 75, 14, 2004
[Cited By]
  1. Ghosh T, Chattopadhyay A, Mandal AC, Pramanik S, Mukherjee S, Kuiri PK, Korean Journal of Chemical Engineering, 38(12), 2549, 2021
참고문헌정보(참고문헌, 인용문헌)는 화학공학소재연구정보센터에 의해 제공되고 있습니다.