Size verification of small and large bubbles in a bubble column was investigated by employing the dynamic gas disengagement (DGD) method and dual electrical resistivity probe (DRP) method, simultancously. The holdups of large and small bubbles in the bubble column in a given operating condition were obtained by means of the DGD method by measuring the pressure drop variation in the column with a variation of time after stopping the gas input into the column. The size and frequency of bubbles were measured by the DRP method in the same operating condition, from which the bubble holdup of each range of size was obtained. The verification of size in determining the large or small bubbles was decided by comparing the holdups of large or small bubbles measured by the DGD method with that measured by the DRP method. Filtered compressed air and tap water were used as a gas and a continuous liquid medium. The diameter and height of the bubble column were 0.102 m and 1.5 m, respectively. The demarcation size between the large and the small bubbles in the bubble column was 4.0~5.0 mm; the demarcation size was about 5.0 mm when the gas velocity was in the relatively low range, but about 4.0 mm when the gas velocity was in the relatively high range, within this experimental conditions.