Partially activated polyacrylonitrile(PAN) composite fiber containing zeolite particle was prepared by using acrylonitrile(AN) as a precursor. Weight average molecular weight(Mw) and polydispersity index of spinning dope was 630,000 and 1.30 respectively. Dry-jet wet spinning technique was used for making PAN composite fiber. During the dry-jet wet spinning process, PAN composite fiber of 35-45 μm in diameter shows increased orientation. Initial elastic modulus of PAN composite fiber containing zeolite particles was 89% of PAN fiber at the same experimental condition. The cyclization and activated state of PAN fiber were confirmed by Fourier transform infrared(FT-IR) spectroscopy and X-ray incorporation of zeolite particles from XRD. Partially activated PAN composite fiber containing zeolite particles is expected to use as an organic-inorganic composite absorbent.