The negative effects on ecosystem are getting serious due to the increase of particulate matters (PM) in the air by the increase of the number of population and the industrial activities. Thus, there have been a lot of environmental policies and researches of air purification system and filter mask to relieve the environmental problem. In this research, activated carbon impregnated cellulose acetate fiber filters produced using an electrospinning technique are studied for air purification. NaCl aqueous solution was used to generate PM and the humid air with NaCl PM was dried using a dehumidifier for the filter performance test. Filtration efficiency was increased with the increase of activated carbons , and acetone adsorption capacity was enhanced.