About The Journal
  Aims and Scope
  Editorial Board
  Submit a Manuscript 
  Subscription Information
Articles & Issues
  Issue
  Search
For Authors
  Instructions to Authors
  Ethics in Publishing
  Peer Review Process
  Author's Checklist
  Copyright Transfer Form
Contact us
 
 
 
 
Search / Korean Journal of Chemical Engineering
Korean Chemical Engineering Research,
Vol.54, No.5, 636-647, 2016
Immobilization of the Thenoyltrifluoroacetone on Sodium Dodecyl Sulfate Modified Magnetite Nanoparticles for Magnetic Solid Phase Extraction of Pb (II) from Water Samples
Sadeghi M, Yekta S, Babanezhad E
Magnetite nanoparticles (Fe3O4 NPs) were synthesized by co-precipitating method under optimized condition. The Fe3O4 NPs coated with sodium dodecyl sulfate-thenoyltrifluoroacetone (Fe3O4 NPs-SDS-TTFA) were then exerted as the magnetic solid phase extraction (MSPE) adsorbent for the extraction process prior to introducing to a flame atomic adsorption spectrometry (FAAS). The synthesized Fe3O4 NPs-SDS-TTFA were applied for the extraction of Pb(II) ions from different water samples. The characterization studies of nanoparticles were performed via scanning electron microscopy-energy dispersive micro-analysis (SEM-EDAX), X-ray diffraction (XRD) and vibrating sample magnetometer (VSM) techniques. The substantial parameters affecting the extraction efficiency were surveyed and optimized. A dynamic linear range (DLR) of 10.400 μg L-1 was obtained and the limit of detection (LOD, n=7) and relative standard deviation (RSD%, n= 6, C=20 μg L-1) were found to be 2.3 μg L-1 and 1.9%, respectively. According to the results, the proposed method successfully applied for the extraction of Pb(II) ions from different environmental water samples and satisfactory results achieved.
Keywords: Magnetite (Fe3O4) NPs; Sodium dodecyl sulfate (SDS); Thenoyltrifluoroacetone (TTFA); Extraction; Pb(II); Water sample
[References]
  1. Ansell RJ, Mosbach K, Analyst, 123(1), 1611, 1998
  2. Jeon C, Park JY, Yoo YJ, Korean J. Chem. Eng., 18(6), 955, 2001
  3. Shao WJ, Chen LH, Lu LL, Luo F, Desalination, 265(1-3), 177, 2011
  4. Rahman I, Furusho Y, Begum ZA, Izatt N, Bruening R, Sabarudin A, Hasegawa H, Microchem J., 98(1), 103, 2011
  5. Baytak S, Turker AR, J. Hazard. Mater., 129(1-3), 130, 2006
  6. Wang ZY, Su YD, Li S, Spectrosc. Spect. Anal., 28(11), 2695, 2008
  7. Tavallali H, Asrari E, Attaran A, Tabandeh M, Int. J. Chem. Tech. Res., 2(3), 1731, 2010
  8. Panda L, Das B, Rao DS, Korean J. Chem. Eng., 28(10), 2024, 2011
  9. Mahmoud ME, Yakout AAA, Abdel H, Osman MM, Bioresour. Technol., 106(1), 125, 2012
  10. Bouranene S, Fievet P, Szymczyk A, Samar MEH, Vidonne A, J. Membr. Sci., 325(1), 150, 2008
  11. Ghaedi M, Shokrollahi A, Niknam K, Niknam E, Najibi A, Soylak M, J. Hazard. Mater., 168(2-3), 1022, 2009
  12. Citak D, Tuzen M, Food. Chem. Toxicol., 48(5), 1399, 2010
  13. Comitre ALD, Reis BF, Talanta, 65(4), 846, 2005
  14. Liang P, Sang H, Anal. Biochem., 380(1), 21, 2008
  15. Rivas RE, Lopez GI, Hernandez CM, Microchim. Acata., 166(3), 355, 2009
  16. Zhang L, Chang X, Li Z, He Q, J. Mol. Struct., 964(1-3), 58, 2010
  17. Bai H, Zhou Q, Xie G, Xiao J, Talanta, 80(5), 1638, 2010
  18. Baysal A, Kahraman M, Akman S, Curr. Anal. Chem., 5(4), 352, 2009
  19. Parham H, Pourreza N, Rahbar N, J. Hazard. Mater., 163(2-3), 588, 2009
  20. Qiu G, Wang Q, Wang C, Lau W, Guo Y, Ultrason. Sonochem., 14(1), 55, 2007
  21. Bhaumik M, Maity A, Srinivasu VV, Onyango MS, J. Hazard. Mater., 190(1-3), 381, 2011
  22. Tataru G, Popa M, Desbrieres J, Int. J. Pharm., 404(1-2), 83, 2011
  23. Kalfa OM, Yalcinkaya O, Turker AR, J. Hazard. Mater., 166(1), 455, 2009
  24. Singh S, Barick KC, Bahadur D, J. Hazard. Mater., 192(3), 1539, 2011
  25. Izatt RM, Bradshaw JS, Bruening RL, Pure. Appl. Chem., 68(1), 1237, 1996
  26. Suh YJ, Do TM, Kil DS, Jang HD, Cho K, Korean Chem. Eng. Res., 53(1), 39, 2015
  27. Akama Y, Ito M, Tanaka S, Talanta, 53(3), 645, 2000
  28. Khajeh M, Laurent S, Dastafkan K, Chem. Rev., 113(10), 7728, 2013
  29. Acar HYC, Garaas RS, Syud F, Bonitatebus P, Kulkarni AM, J. Magn. Magn. Mater., 293(1), 1, 2005
  30. Jeng HT, Guo GY, Phys. Rev. B, 65(9), 094429, 2002
  31. Tartaj P, del Puerto MM, Veintemillas-Verdaguer S, Gonzalez-Carreno T, Serna C, J. Phys. D-Appl. Phys., 36(13), 182, 2003
  32. Cornell RM, Schwertmann U, Iron oxides: Structure, Properties, Reactions, Occurrence, and Uses, 2nd ed.,Wiley-VCH, Weinheim(2003).
  33. Muller R, Dutz S, Habisreuther T, Zeisberger M, J. Magn. Magn. Mater., 323(10), 1223, 2011
  34. Kassaee MZ, Motamedi E, Majdi M, Chem. Eng. J., 172(1), 540, 2011
  35. Zhang J, Zhai S, Li S, Xiao Z, Song Y, Qingda A, Tian G, Chem. Eng. J., 215-216(1), 461, 2013
  36. Sun ZX, Su FW, Forsling W, Samskog PO, J. Colloid Interface Sci., 197(1), 151, 1998
  37. Tan Y, Chen M, Hao Y, Chem. Eng. J., 191(1), 104, 2012
  38. Karimi MA, Hatefi-Mehrjardi A, Mohammadi SZ, Mohadesi A, Mazloum-Ardakani M, Hormozi Nezhad MR, Askarpour Kabir A, J. Iran. Chem. Soc., 9(2), 171, 2012
  39. Mashhadizadeh MH, Amoli-Diva M, Shapouri MR, Afruzi H, Food Chem., 151(1), 300, 2014
  40. Buendia S, Cabanas G, Alvarez-Lucio G, Montiel-Sanchez H, Navarro-Clemente ME, Corea M, J. Colloid Interface Sci., 354(1), 139, 2011
  41. Tarley CRT, Ferreira SLC, Arruda MAZ, Microchem J., 77(2), 163, 2004
  42. Patterson A, Phys. Rev., 56(10), 978, 1939
  43. Ngomsik AF, Bee A, Siaugue JM, Talbot D, Cabuil V, Cote G, J. Hazard. Mater., 166(2-3), 1043, 2009
  44. Saracoglu S, Elci L, Anal. Chim. Acta., 452(1), 77, 2002
  45. Ferreira SLC, lemos VA, Santelli RE, Ganzarolli E, Curtius AJ, Microchem J., 68(1), 41, 2001
  46. Costa ACS, Lopesa L, Korn MGA, Portela JG, J. Braz. Chem. Soc., 13(5), 674, 2002
  47. Ozmen M, Can K, Arslan G, Tor A, Cengeloglu Y, Ersoz M, Desalination, 254(1-3), 162, 2010
  48. Zhu X, Chang X, Cui Y, Zou X, Yang D, Hu Z, Microchem J., 86(2), 189, 2007
  49. Candir S, Narin I, Soylak M, Talanta, 77(1), 289, 2008
  50. Singh BK, Kumar DN, Garg BS, Indian J. Chem. Technol., 12(4), 413, 2005
  51. Sacmaci S, Kartal S, Sacmaci M, Fresen. Environ. Bull., 21(6a)
  52. Moghimi A, Hashemi-Moghaddam H, J. Chem. Health Risks., 5(2), 105, 2015
  53. Rahnama R, Ghadiri R, J. Braz. Chem., 26(8), 1642, 2015
  54. Moghimi A, Ghiasi R, Behrouzinia S, “Extraction Pb(II) by (Z)-Furan-2-Carbaldehyde Thiosemicarbazone Adsorbed on Surfactant Coated Alumina Before Determination by FAAS,” IJFPS., 1(4), 74-78(2011).
  55. Divrikli U, Kartal AA, Soylak M, Elci L, J. Hazard. Mater., 145(3), 459, 2007
  56. Barbosa AF, Segatelli MG, Pereira AC, Santos AS, Kubota LT, Luccas PO, Tarley CR, Talanta, 71(4), 1512, 2007
  57. Venkatesh G, Singh AK, Venkataramani B, Microchim. Aata., 144(4), 233, 2004
  58. Mansour SF, J. Magn. Magn. Mater., 323(13), 1735, 2011
참고문헌정보(참고문헌, 인용문헌)는 화학공학소재연구정보센터에 의해 제공되고 있습니다.